Draft Data Validation Plan Review Form Page 11
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29Draft Data Validation PRF-Tier II
Date: March 2, 2004
Page 11
Revision: 4.0
4.0
Volatile Organic Data Review - Target Compound Identification
4.2
Check the sample compound spectra against spectral
data of the standard. All ions in the standard mass
spectra at a relative intensity of 10% must also be in the
identified sample compound.
Action: Use this information in conjunction with the mass spectral
analysis information to qualify data.
If target compound
identification is in error, qualify that compound as “R.”
4.3
Check the sample compound spectra against spectral
data of the standard. The relative intensity of the ions in
the sample must agree within +/- 20% of the value
obtained from the standard spectrum.
Action: Use this information in conjunction with the mass spectral
analysis information to qualify data. If target compound
identification is in error, qualify that compound as “R.”
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