Quality Assurance Project Plan Including Sampling And Analysis Plan Page 24
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67Hunters Point Shipyard Parcel F ESTCP Demonstration Plan
Appendix A: Quality Assurance Project Plan
sampling. All field records and documentation must comply with the documentation requirements defined
in this section. Copies of all field data collection forms are provided in Attachment 1.
Field data and observations will be recorded in real time on activity-specific data forms that are bound
into the logbooks. Completion of a sample collection form for each sample is the responsibility of the
appropriate Research Studies Leader. The information recorded for each sample includes, as appropriate:
•
Unique sample ID number and description
•
Date and time of collection
•
Identification of person who collected the sample
•
Identification of person recording field data (if different than the collector)
•
Sample location (Lat/Long or State Plane)
•
Sampler type
•
Sampling procedures, sample volume and receiving container
•
Storage conditions from sampling to aliquotting or shipment.
A.2.7.4
Laboratory Documentation
Documentation of all laboratory activities is critical for tracking data and evaluating the success of any
activity. It is expected that each laboratory maintains written policies that define documentation
requirements and procedures. Laboratory documentation requirements at BDO are defined in the
laboratory QA Manual and SOPs. Required documentation includes, but is not limited to, the following:
•
Calibration and maintenance records for all instruments and equipment involved in the
collection of environmental data.
•
Preparation of calibration standards, spiking solutions, and dosing solutions such that each
unique preparation can be tracked to the original (neat) material.
•
Lot numbers for all standards, stock solutions, reagents, and solvents.
•
All sample processing or preparation for testing such that it is traceable to sample receipt
records.
•
All sample analyses and results of analyses. All rejected data are accompanied by
explanations of the failure and the corrective action.
•
All data reduction formulas such that reported data can be reproduced from the raw data.
A.2.7.5
Contents of Data Packages
Laboratories at Stanford, UMBC, and ERDC will generate full data packages for 20% of the samples
analyzed and summary data packages for 80% of the sample analyzed. BDO laboratory will generate a
full data package for 100% of the samples analyzed. The full data package contains all information
required for validation (Section A.5.0 discusses data validation requirements). The full data packages
must contain any of the following elements that are applicable to the analysis because the data will be
validated:
•
Title page;
•
Table of contents;
Page A-
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of A-67
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