Quality Assurance Project Plan Including Sampling And Analysis Plan Page 67
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67Hunters Point Shipyard Parcel F ESTCP Demonstration Plan
Appendix A: Quality Assurance Project Plan
Table A-13. Level III Data Validation Assessment Parameters
Criteria
PCBs (GC)
X
Holding times
Instrument tunes
Initial and continuing
X
calibrations
Blanks
X
(5X/10X rule)
LCS/
Laboratory set limits
Surrogates
X
MS/MSD
X
Duplicates
Internal standard area
performance
Target compound
X
retention times
Instrument performance
X
Interference with
X
compound quantification
Page A-
67
of A-67
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