Quality Assurance Project Plan Including Sampling And Analysis Plan Page 62
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67Hunters Point Shipyard Parcel F ESTCP Demonstration Plan
Appendix A: Quality Assurance Project Plan
Table A-6. Container, Sample Size, Preservation, and Shipping Information for the ESTCP
DP
Sample Container
Min.
Sample
Number, Type,
Sample
Preser-
Holding
Receiving Laboratory and
(a)
Sample Type
Size
Size
vation
Time
Sample Custodian
Clams
500 mL vented
One
In cooler
24 h from
Stanford University
polyethylene jar
clam
with ice,
collection to
Dept. Civil & Environmental
but no
depuration
Engineering, B-55
direct ice-
Stanford, CA 94305
clam
Attn: Dennis Smithenry
contact.
(650) 723-8574
Depurated
20 mL pre-cleaned
One
Frozen
1 yr/40 d
U.S. Army Engineer Research
Shucked Whole
scintillation vial
whole
and Development Center
(-10°C)
Clam Tissues for
clam
(ERDC)
Splitting and
tissue
3909 Halls Ferry Rd.
Analysis
Vicksburg, MS 39180-6199
Attn: Todd Bridges
(601) 634-3626
Depurated
20 mL pre-cleaned
2 g
Frozen
1 yr/40 d
Battelle
Shucked Whole
scintillation vial
homo-
397 Washington Street
(-10°C)
Clam Tissues for
genate
Duxbury, MA 02332
Archive
Attn: Carole P-McCarthy
(781) 952-5232
SPMDs
Original sample
1
1 yr/40 d
Stanford University
4°±2°C
containers from
(once
supplier or 4 oz.
ampoule is
(b)
pre-cleaned wide
open)
mouth glass
Sediment Cores
2-inch diameter
12
TOC (1 yr)
Stanford University
4°±2°C
butyrate core tube
inches
PCBs (1
(1.5 ft. long)
yr/40d)
Benthic
in 4% formaldehye
N/A
3 yr/(N/A)
ERDC
4°±2°C
Community
solution in 500 mL
Samples
polyethylene jars
Amphipod
20 mL pre-cleaned
200 mg
Frozen
1 yr/40 d
ERDC
Sample for
scintillation vial
(-10°C)
Splitting and
Analysis
Amphipod
20 mL pre-cleaned
100 mg
Frozen
1 yr/40 d
Battelle
Sample for
scintillation vial
homo-
(-10°C)
Archive
genate
Surface Water
8 oz. pre-cleaned
One
1 yr/40 d
University of Maryland
4°±2°C
Samples—Filter
wide mouth glass
Baltimore County
Papers
1000 Hilltop Circle
Baltimore, MD 21250
Attn: Upal Ghosh
410-455-8665
Surface Water
50mm x 300mm
400 mL
1 yr/40 d
University of Maryland
4°±2°C
Samples—XAD
Glass Column
XAD
Resin Columns
Capped after
Collection
(a)
Holding time: yr = year; d = day; h = hour; x/y = days from collection to extraction/days from extraction to
analysis.
(b)
SPMD samples can be stored for an undetermined period of time. Once SPMDs have undergone dialysis,
the hexane extracts sealed in ampoules can also be stored under refrigeration for an undetermined period of
time. (Personal communication, Terri Spencer, EST Laboratory, 2004).
Page A-
62
of A-67
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